Collect. Czech. Chem. Commun. 2010, 75, 971-980
https://doi.org/10.1135/cccc2010046
Published online 2010-09-22 08:35:17

Synthesis, characterization, and thermal properties of benzylammonium pentaborate [C6H5CH2NH3][B5O6(OH)4]

Michael A. Becketta,*, Peter N. Hortonb, Michael B. Hursthouseb, James L. Timmisa and K. Sukumar Varmac

a School of Chemistry, Bangor University, Bangor, LL57 2UW, UK
b School of Chemistry, Southampton University, Southampton, SO16 1BJ, UK
c Pilkington Building Products R and D, European Technical Centre, Lathom, Lancashire, L40 3UF, UK

References

1. de A. A. Soler-Illia G. J., Sanchez C., Lebeau B., Patarin J.: Chem. Rev. 2002, 102, 4093. <https://doi.org/10.1021/cr0200062>
2a. Akella A., Keszler D. A.: Mater. Res. Bull. 1995, 30, 105. <https://doi.org/10.1016/0025-5408(94)00113-8>
2b. Dotsenko V. P., Efryshina N. P., Berezovskaya I. V.: Mater. Lett. 1996, 28, 517. <https://doi.org/10.1016/0167-577X(96)00114-0>
3a. Cook W. R., Jr., Jaffe H.: Acta Crystallogr. 1957, 10, 705. <https://doi.org/10.1107/S0365110X57002431>
3b. Graja A.: Physica Status Solidi 1968, 27, K93. <https://doi.org/10.1002/pssb.19680270237>
3c. Touboul M., Betourne E.: Solid State Ionics 1993, 63-65, 340. <https://doi.org/10.1016/0167-2738(93)90126-N>
4a. Chen C., Wu B., Jiang A., You G.: Sci. Sin., Ser. B 1985, 235.
4b. Chen C., Wu Y., Jiang A., Wu B., You G., Li R., Lin S.: J. Opt. Soc. Am. B 1989, 6, 616. <https://doi.org/10.1364/JOSAB.6.000616>
4c. Yang S., Li G., Tian S., Liao F., Lin J.: Cryst. Growth Des. 2007, 7, 1246. <https://doi.org/10.1021/cg0606794>
5. Schubert D. M., Visi M. Z., Knobler C. B.: Inorg. Chem. 2008, 47, 2017. <https://doi.org/10.1021/ic7020098>
6. Hellor G.: J. Inorg. Nucl. Chem. 1968, 30, 2734.
7a. Visi M. Z., Knobler C. B., Owen J. J., Khan M. I., Schubert D. M.: Cryst. Growth Des. 2006, 6, 538. <https://doi.org/10.1021/cg0504915>
7b. Yang Z. L., Yang S. H., Li G. B., Tian S. J., Liao F. H., Lin J. H.: Acta Phys.-Chim. Sin. 2007, 23, 285.
8. Schubert D. M., Visi M. Z., Khan S., Knobler C. B.: Inorg. Chem. 2008, 47, 4740. <https://doi.org/10.1021/ic800068t>
9. Schubert D. M., Visi M. Z., Knobler C. B.: Inorg. Chem. 2000, 39, 2250. <https://doi.org/10.1021/ic000217u>
10. Liu Z. H., Li L. Q., Zhang W. J.: Inorg. Chem. 2006, 45, 1430. <https://doi.org/10.1021/ic051580+>
11a. Beckett M. A., Coles S. J., Light M. E., Fischer L., Steifvater-Thomas B. M., Varma K. S.: Polyhedron 2006, 25, 1011. <https://doi.org/10.1016/j.poly.2005.11.032>
11b. Beckett M. A., Bland C. C., Coles S. J., Horton P. N., Hursthouse M. B., Varma K. S.: Inorg. Chem. 2007, 46, 3801. <https://doi.org/10.1021/ic700433e>
11c. Beckett M. A., Horton P. N., Knox D. A., Timmis J. L.: Dalton Trans. 2010, 39, 3944. <https://doi.org/10.1039/b927072h>
12. CCDC 776543 contains the supplementary crystallographic data for this paper. These data can be obtained free of charge via www.ccdc.cam.ac.uk/conts/retrieving.html (or from the Cambridge Crystallographic Data Centre, 12, Union Road, Cambridge, CB2 1EZ, UK; fax: +44 1223 336033; or [email protected]).
13. Hooft R.: Collect, Data Collection Software. Nonius BV, Delft 1998.
14. Otwinowski Z., Mino W.: Methods Enzymol. 1997, 276, 307. <https://doi.org/10.1016/S0076-6879(97)76066-X>
15. Sheldrick G. M.: SADABS, Program for Area Detector Adsorption Correction. University of Göttingen, Göttingen 1996.
16. Sheldrick G. M.: Acta Crystallogr., Sect. A: Found. Crystallogr. 2008, 64, 112. <https://doi.org/10.1107/S0108767307043930>
17a. Rademeyer M.: Acta Crystallogr., Sect. E 2006, 62, m269. <https://doi.org/10.1107/S1600536806000201>
17b. Amini M. M., Nasiri S., Ng S. W.: Acta Crystallogr., Sect. E 2007, 63, o1361. <https://doi.org/10.1107/S1600536807007465>
17c. Rademeyer M.: Acta Crystallogr., Sect. E 2003, 59, o1860. <https://doi.org/10.1107/S1600536803024243>
17d. Lee C., Harrison T. A.: Acta Crystallogr., Sect. E 2003, 59, m1151. <https://doi.org/10.1107/S1600536803026242>
18a. Doerrer L. H., Green M. L. H.: J. Chem. Soc., Dalton Trans. 1999, 4325. <https://doi.org/10.1039/a905892c>
18b. Beckett M. A., Brassington D. S., Light M. E., Hursthouse M. B.: J. Chem. Soc., Dalton Trans. 2001, 1768. <https://doi.org/10.1039/b100981h>
18c. Parks D. J., Piers W. E., Parvez M., Atencio R., Zanworotko M. J.: Organometallics 1998, 17, 1369. <https://doi.org/10.1021/om9710327>
18d. Beckett M. A., Brassington D. S., Coles S. J., Hursthouse M. B.: Inorg. Chem Commun. 2000, 3, 530. <https://doi.org/10.1016/S1387-7003(00)00129-5>
19a. Beckett M. A., Bennett E. L., Horton P. N., Hursthouse M. B.: J. Organomet. Chem. 2010, 695, 1080. <https://doi.org/10.1016/j.jorganchem.2009.09.026>
19b. Beckett M. A., Strickland G. C., Varma K. S., Hibbs D. E., Hursthouse M. B., Abdul Malik K. M.: Polyhedron 1995, 14, 2623. <https://doi.org/10.1016/0277-5387(95)00130-K>
20. Etter M. C.: Acc. Chem. Res. 1990, 23, 120. <https://doi.org/10.1021/ar00172a005>
21a. Freyhardt C. C., Wiebcke M., Felsche J., Engelhardt G.: Z. Naturforsch., B: Chem. Sci. 1993, 48, 978.
21b. Beckett M. A., Knox D. A.: Templating Pentaborate(–1) Anions by Non-Metal Cations. Presented at IMEBORON XIII, Platja d’Aro, September 21–25, 2008.
22. Freyhardt C. C., Wiebcke M., Felsche J., Engelhardt G.: J. Inclusion Phenom. Mol. Recogn. Chem. 1994, 18, 161. <https://doi.org/10.1007/BF00705819>